Instrument/equipment Core/facility: Yale University Cleanroom

Dry and plasma etching

Building:

Becton Engineering and Applied Science Center, 5th floor

About the instruments

Yale’s cleanroom is equipped with multiple dry etchers and a wide variety of process gases. It is capable of etching metals, semiconductors, and organic films at controllable rates with high selectivity. The cleanroom is also capable of filling niche applications such as cryo and Bosch deep silicon etching and oxygen surface cleaning.

The Oxford 100 and DRIE both require four-inch wafers. When etching smaller samples, it is recommended to mount samples to a four-inch carrier wafer. The cleanroom supplies Crystalbond 555-HMP for this purpose, but photoresist, Santovac 5, and AIT Cool-Grease are all acceptable alternatives.

For wet etching capabilities, see the wet chemistry hoods.

Available to Yale researchers & external researchers

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Equipment

Cleanroom_plasmafab100

Oxford 100 ICP RIE

The Oxford 100 is critical to several research applications at Yale. It has the largest variety of etch gases available and can handle the largest variety of research samples, including III-V materials, semiconductors, and select metals.  This load-locked system requires samples to either be 4-inch wafers or mounted on 4-inch wafers. In addition to deep silicon etching, this system is also capable of etching a limited selection of dielectrics and other materials.

  • Tool manager: Yong Sun
  • Gas selection: Cl2, BCl3, CH4, SF6, CHF3, CF4, O2, Ar, H2
  • Coil and bias powers: 600 W and 3000 W
  • Compatible materials*: Si, SiO, SiN, GaAs, GaN, Al, AlN, AlO, LiNbO, InP, Parylene, HBN, FTO, MoS2, carbon, Ni, SiC, +PR, -PR, PMMA
  • Banned materials*: Au, Ag, Pt, Cu, magnetics
    * Due to the ever-changing nature of research and the sensitive nature of the equipment, these lists are incomplete. Please contact a staff member to discuss etch plans before attempting to introduce a new material to the system.
  • Internal rate: $64.00/hour
Cleanroom_Oxford80

Oxford 80+ ICP RIE

The Oxford Plasmalab 80 Plus Inductively Coupled Plasma Reactive Ion Etcher (ICP RIE) provides etching capability for superconductors and select other “clean” materials. It uses fluorine chemistry along with oxygen and argon to etch films on the nanometer-to-micron scale. This open-load system has a 2-inch graphite clamp for use with helium backside cooling as well as replaceable quartz and graphite platens for different etch chemistries.

  • Tool manager: Yong Sun
  • Gas selection: O2, SF6, CF4, CHF3, Ar
  • Coil and bias powers: 600 W and 600 W
  • Allowed materials*: Si, SiO, SiN, Nb, NbN, Ta, Ge, positive resist, PMMA
  • Banned materials*: Au, Ag, Pt, Cu, most other materials.
    * Due to the ever-changing nature of research and the sensitive nature of the equipment, these lists are incomplete. Please contact a staff member to discuss etch plans before attempting to etch a new material.
  • Internal rate: $64.00/hour
Cleanroom_DRIE

Oxford Cryo Bosch DRIE

The Oxford Cryo Bosch Deep Reactive Ion Etcher (DRIE) is a specialized ICP RIE etcher. It can perform high aspect-ratio etches in silicon on the scale of hundreds of microns. It accomplishes this using either the Bosch multiplex process or the cryogenic etch process. Common applications for this tool involve microfluidics, PDMS mold development, and MEMS applications. This load-locked system requires samples to either be 4-inch wafers or mounted on 4-inch wafers. In addition to deep silicon etching, this system is also capable of etching a limited selection of dielectrics and other materials.

  • Tool manager: Yong Sun
  • Gas selection: O2, SF6, C4F8, Ar, CF4, CHF3
  • Coil and bias powers: 600 W and 3000 W
  • Allowed materials*: Si, SiO, SiN, Al, Al2O3, AlN, Ni, Cr, Positive resist, PMMA
  • Banned materials*: Most other materials.
    * Due to the ever-changing nature of research and the sensitive nature of the equipment, these lists are incomplete. Please contact a staff member to discuss etch plans before attempting to etch a new material.
  • Internal rate: $64.00/hour
Cleanroom_Autoglow

AutoGlow 200 Plasma Cleaner

The AutoGlow 200 is a basic plasma asher, enabled with O2 and Ar for substrate cleaning, descumming, and surface treatment. It can operate between 50 W and 300 W, typically at 300 mTorr. The two-level table design creates separate zones for high power film removal and low power cleaning. Note that the relationship between power and etch rate aren’t necessarily linear.

  • Tool manager: Yong Sun
  • RIE power: 50 W - 300 W
  • Allowed materials: Most materials. Check with a staff member before using.
  • Internal rate: included with cleanroom access
Cleanroom_Xactix

Xactix XeF2 Silicon Etcher

Ideal for MEMS device release, the XactiX XeF2 uses vapor to spontaneously react with silicon in a high selectivity etch process. It etches isotropically and is ideal for situations where under ten percent of the sample is exposed.
 

  • Tool manager: Yong Sun
  • Internal rate: included with cleanroom access